HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 3-chloro-4-hydroxyphenylacetate → 3-Chloro-4-(3'-chloro-4'-isobutoxybenzyloxy) phenylacetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 3-chloro-4-hydroxyphenylacetate | HCID 92625 | — |
| Edukt | 3-Chloro-4-isobutyoxybenzyl chloride | HCID 12347939 | — |
| Lösungsmittel | Methanol--water (1/1) | HCID 22242641 | — |
| Produkt | 3-Chloro-4-(3'-chloro-4'-isobutoxybenzyloxy) phenylacetic acid | HCID 53758658 | — |
Reaktionsschritte
The procedure of Example (1) (e) was repeated wherein 3-chloro-4-isobutyoxybenzyl chloride was reacted with methyl 3-chloro-4-hydroxyphenylacetate to yield 3-chloro-4-(3'-chloro-4'-isobutoxybenzyloxy) phenylacetic acid (52.4yield), m.p. 127.5°-129° C. (methanol-water).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04221919 |
| Quelldatensatz | uspto-grants-1980_09 |
| ORD ID | ord-ed19a95cc9c14b48830e71430588f306 |
| Quellennotiz | uspto-grants-1980_09 |