HRID276075

反应详情

EQUATION

反应方程式

HRID 276075 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Sodium borohydride (0.48 g) was added to a solution of 4.96 g of 4-phenoxybenzaldehyde in 20 ml of ethanol, and the mixture was stirred at room temperature for 1.5 hours. After the completion of the concentration, the residue was extracted with tert-butylmethyl ether and with water. The organic layer was concentrated to give 4.84 g of 4-phenoxybenzyl alcohol.

WORKUP

后处理

  1. concentrationAfter the completion of the concentration
  2. extractionthe residue was extracted with tert-butylmethyl ether and with water
  3. concentrationThe organic layer was concentrated