HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 18316937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 85394088 | HCID 85394088 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18316937 | HCID 18316937 | — |
Reaction Steps
A more particular subject of the invention is a process characterized in that 1-(3-pyridinyl)-ethanone O-[(4-methylphenyl) sulphonyl] oxime is subjected to the action of methanol and sodium methylate in order to obtain 3-(2H-azirin-3-yl)-pyridine which is subjected to the action of oxalic acid in order to obtain β,β-dimethoxy-2-(3-pyridinyl)ethyl)-amine which is subjected to the action of formamide in order to obtain N-[β,β-dimethoxy-2-(3-pyridinyl)ethyl]-formamide which is subjected to a cyclization in order to obtain the sought product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353108B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-c559ca488bd94680b8c0e49f0d5bf0a6 |
| Source note | uspto-grants-2002_03 |