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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 276107Generated: October 30, 2026

Sodium Methoxide → HCID 18316937, compound

https://huagongshe.com/reaction/276107

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium MethoxideHCID 10942334—
ReactantHCID 85394088HCID 85394088—
SolventMethanolHCID 887—
ProductHCID 18316937HCID 18316937—

Reaction Steps

A more particular subject of the invention is a process characterized in that 1-(3-pyridinyl)-ethanone O-[(4-methylphenyl) sulphonyl] oxime is subjected to the action of methanol and sodium methylate in order to obtain 3-(2H-azirin-3-yl)-pyridine which is subjected to the action of oxalic acid in order to obtain β,β-dimethoxy-2-(3-pyridinyl)ethyl)-amine which is subjected to the action of formamide in order to obtain N-[β,β-dimethoxy-2-(3-pyridinyl)ethyl]-formamide which is subjected to a cyclization in order to obtain the sought product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06353108B1
Source datasetuspto-grants-2002_03
ORD IDord-c559ca488bd94680b8c0e49f0d5bf0a6
Source noteuspto-grants-2002_03