HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 18316937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 85394088 | HCID 85394088 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18316937 | HCID 18316937 | — |
Reaction Steps
100 g of 1-(3-pyridinyl)-ethanone O-[(4-methylphenyl)sulphonyl]-oxime is introduced at 20° C. under a nitrogen atmosphere into a solution containing 400 ml of anhydrous methanol and 23.45 g of sodium methylate. Agitation is carried out for 2 hours at 20˜22° C. and a suspension containing the sought product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353108B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-efaf125244ff4aa980cb0bc15a95ac5e |
| Source note | uspto-grants-2002_03 |