HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 2,8-Dichloro-10,11-dihydro-11-(4-pyridyl)dibenz[b,f][1,4]oxazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | 2,8-Dichloro-11-(1,2,3,6-tetrahydro-1-methyl-4-pyridyl)-dibenz[b,f][1,4]oxazepine | HCID 23342647 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2,8-Dichloro-10,11-dihydro-11-(4-pyridyl)dibenz[b,f][1,4]oxazepine | HCID 23342665 | — |
Reaction Steps
A 20.0 g. portion of 2,8-dichloro-11-(4-pyridyl)-dibenz[b,f][1,4]oxazepine (Example 2), 10.0 g. of lithium aluminum hydride and 800 ml. of ether are reacted as described in Example 3, yielding 2,8-dichloro-10,11-dihydro-11-(4-pyridyl)-dibenz[b,f][1,4]oxazepine, mp. 202°-205° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04221714 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-6378e3ea413148dc9987027b6b2a6ede |
| Source note | uspto-grants-1980_09 |