HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-methylpropane → HCID 54520243, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-methylpropane | HCID 6555 | — |
| Reactant | HCID 178428752 | HCID 178428752 | — |
| Product | HCID 54520243 | HCID 54520243 | 32% |
Reaction Steps
(R)-4-Isopropyl-2-(2-methyl-4-nitrophenylimino)-2,3,4,5-tetrahydro-1,3-thiazine Method C3a) was reacted with isobutyl bromide in a manner analogous to Method D2a to yield (4R)-3-isobutyl-4-isopropyl-2-(2-methyl-4-nitrophenylimino)tetrahydro-2H-1,3-thiazine (0.081 g, 32%). TLC (33% EtOAc/hex) Rf0.76.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353006B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-53c8216a93a94c1b826138981909adc8 |
| Source note | uspto-grants-2002_03 |