Thionyl Chloride → HCID 86590171, compound

HRID 276317Notes

Reaction equation

CC(N)CC.O[CH2:7][CH2:8][NH:9][CH:10]([CH2:12][CH3:13])[CH3:11].O=S(Cl)[Cl:16]>>[Cl-:16].[Cl:16][CH2:7][CH2:8][NH2+:9][CH:10]([CH2:12][CH3:13])[CH3:11]

Participants

Reactant 3

HCID 24386Thionyl Chloride

HCID 24874Sec-Butylamine

HCID 984292-[(1-Methylpropyl)amino]ethanol

Product 1

HCID 86590171HCID 86590171, compound

Procedure

2-Butylamine was converted to N-(2-hydroxyethyl)-N-(2-butyl)amine according to Method B5a. The amine was reacted with SOCl2 according to Method B7a to give N-(2-chloroethyl)-N-(2-butyl)ammonium chloride. The chloroethylamine was reacted with 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to give to give 2-(2-methyl-4-nitrophenylimino)-3-(2-butyl)-1,3-thiazolidine.

Sources & evidence

ORD record: ord-692ffba009904fccb5d51d92e7160374
Source dataset: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06353006B1

Reaction notes

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