HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86590171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Sec-Butylamine | HCID 24874 | — |
| Reactant | 2-[(1-Methylpropyl)amino]ethanol | HCID 98429 | — |
| Product | HCID 86590171 | HCID 86590171 | — |
Reaction Steps
2-Butylamine was converted to N-(2-hydroxyethyl)-N-(2-butyl)amine according to Method B5a. The amine was reacted with SOCl2 according to Method B7a to give N-(2-chloroethyl)-N-(2-butyl)ammonium chloride. The chloroethylamine was reacted with 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to give to give 2-(2-methyl-4-nitrophenylimino)-3-(2-butyl)-1,3-thiazolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353006B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-692ffba009904fccb5d51d92e7160374 |
| Source note | uspto-grants-2002_03 |