HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-methylpropane → 2-(2-Methyl-4-nitrophenylimino)-3-isobutyl-5,5-dimethyl-1,3-thiazolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-methylpropane | HCID 6555 | — |
| Reactant | HCID 178428744 | HCID 178428744 | — |
| Product | 2-(2-Methyl-4-nitrophenylimino)-3-isobutyl-5,5-dimethyl-1,3-thiazolidine | HCID 18316237 | — |
Reaction Steps
2-Methyl-2-hydroxypropylamine was reacted with SOCl2 followed by 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to afford 2-(2-methyl-4-nitrophenylimino)-5,5-dimethyl-1,3-thiazolidine. The thiazolidine was reacted with isobutyl bromide according to Method D2g to afford 2-(2-methyl-4-nitrophenylimino)-3-isobutyl-5,5-dimethyl-1,3-thiazolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353006B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-ca5b5cc8c45943699b38e3393ed9b4ad |
| Source note | uspto-grants-2002_03 |