huagongshe.com
HRID27669

反应详情

EQUATION

反应方程式

HRID 27669 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1cc(C)sc1NC(=O)C(C)C
HCID23341602

未命名化合物

结构：O.O.[I-].[Li+]
HCID23688289

Lithium iodide--water (1/1/2)

H4ILiO2

PRODUCTS

生成物

1
结构：Cc1ccc(NC(=O)C(C)C)s1
HCID23341628

2-Methyl-N-(5-methylthiophen-2-yl)propanamide

C9H13NOS

收率 54%

PROCEDURE

实验过程

The ester from Example 48 was treated with lithium iodide dihydrate as in Example 42 to give the expected decarboxylated product, N-(5-methyl-2-thienyl)-2-methylpropanamide, m.p. 96°-97° C. in 54% yield.