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HRID2767

反应详情

EQUATION

反应方程式

HRID 2767 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1cc2nc(Cl)ccc2s1
HCID22017299

未命名化合物

结构：Cl.N#Cc1cc(CN2CC[C@H](N)C2=O)cs1
HCID22883629

未命名化合物

PRODUCTS

生成物

1
结构：N#Cc1cc(CN2CC[C@H](NS(=O)(=O)c3cc4nc(Cl)ccc4s3)C2=O)cs1
HCID54379487

未命名化合物

PROCEDURE

实验过程

The title compound is prepared from 4-(3-(S)-amino-2-oxo-pyrrolidin-1-ylmethyl)-thiophene-2carbonitrile hydrochloride as described in EXAMPLE 1, Part E using 5-chlorothieno[3,2-b]pyridine-2-sulfonyl chloride in place of benzo[b]thiophene-2-sulfonyl chloride. The product is triturated with Et2O/CH2Cl2 /hexanes to give a white solid.

WORKUP

后处理

  1. customThe product is triturated with Et2O/CH2Cl2 /hexanes
  2. customto give a white solid