HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 53683895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54106428 | HCID 54106428 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53683895 | HCID 53683895 | — |
Reaction Steps
To a solution of t-butyl (S)-5-(3-methoxycarbonyl-1H-pyrazol-1-yl)-2-(t-butoxycarbonylamino)-pentanoate (0.84 g, 0.21 mmol) in CH2Cl2 (20 mL) at 0° C. is bubbled HCl gas for 30 minutes. Afterward, the solution is warmed to room temperature over 30 minutes. Evaporation of solvent yields (S)-5-(-3-methoxycarbonyl-1H-pyrazol-1-yl)-2-aminopentanoic acid.HCl as a gray-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353017B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-63454fb629c943d78b8902eb078ef3bd |
| Source note | uspto-grants-2002_03 |