HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178426378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Ethyl 4-(p-tolylamino)-1,2,3-triazole-5-carboxylate | HCID 178470433 | — |
| Solvent | Propan-2-one--water (1/1) | HCID 18366337 | — |
| Product | HCID 178426378 | HCID 178426378 | 96.6% |
Reaction Steps
Hydrolysis of ethyl 4-(p-tolylamino)-1,2,3-triazole-5-carboxylate (4.5 g) with aqueous sodium hydroxide as described in example 1c, afforded 3.85 g (96%) of acid of mp (acetone-water) 144° C., (Found; C, 55.32; H, 4.86; N, 25.64; C10H10N4O2 requires; C, 55.04; H, 4.62; N, 25.77%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04223032 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-7a8a62db10d84e3bb41e563a15627eb2 |
| Source note | uspto-grants-1980_09 |