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Ethyl bromoacetate → Ethyl N-(3-benzoylphenyl)-glycinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl bromoacetate | HCID 7748 | — |
| 反応物 | Methanone, (3-aminophenyl)phenyl- | HCID 17817 | — |
| 生成物 | Ethyl N-(3-benzoylphenyl)-glycinate | HCID 23341870 | 66% |
反応手順
4.5 g Ethyl N-(3-benzoylphenyl)-glycinate, obtained at a 66% yield from 3-aminobenzophenone and ethyl bromoacetate by an analogous procedure to that of Example 1, are heated in the presence of 10 ml dimethyl sulphate and 2 ml water to 100° C. for 11/2 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04223039 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-7f04aaabcb704bf68611636b6f828286 |
| 出典メモ | uspto-grants-1980_09 |