HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → N-tritylethylenediamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Ninhydrin | HCID 10236 | — |
| Edukt | N-(4-monomethoxytrityl)ethylenediamine | HCID 13871404 | — |
| Edukt | N-(4,4'-dimethoxytrityl)ethylenediamine | HCID 18314385 | — |
| Lösungsmittel | Dichloromethane methanol | HCID 21226129 | — |
| Produkt | N-tritylethylenediamine | HCID 2794294 | — |
Reaktionsschritte
C21H22N2 (288.42); RF=0.21 (DCM/MeOH 5:1, v/v); spot stains with ninhydrin spray or with HCl vapour); N-(4-monomethoxytrityl)ethylenediamine; C22H24N2O (332.45); RF=0.21 (DCM/MeOH 5:1, v/v); spot stains with ninhydrin spray or with HCl vapour); N-(4,4′-dimethoxytrityl)ethylenediamine; C23H26N2O2 (362.48); RF=0.22 (DCM/MeOH 5:1, v/v); spot stains with ninhydrin spray or with HCl vapour).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06355726B1 |
| Quelldatensatz | uspto-grants-2002_03 |
| ORD ID | ord-45976f6eee0042eead84adfd86219e10 |
| Quellennotiz | uspto-grants-2002_03 |