HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → HCID 22628911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | HCID 22628886 | HCID 22628886 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22628911 | HCID 22628911 | — |
Reaction Steps
Similar to Example 1, 4.75 g (5 mmol) of PF 1022 in 10 ml of THF were reacted with 100 ml of a 1 M solution of borane and worked-up. Chromatography gave 0.75 g (17% of theory) of tetrareduction product 8,20-dibenzyl-5,11,17,23-tetraisobutyl-2,4,10,14,16,22-hexamethyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosan-6,12,18,24-tetraone as a light-yellow viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06355615B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-7ec0bba78c1148959448e9628caeb4a6 |
| Source note | uspto-grants-2002_03 |