Chloroform → 123334-93-0

HRID 277470Notes

Reaction equation

HRID 277470 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6](C=O)=[CH:7][CH:8]=1.[CH:11]1([NH2:17])[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1.[CH:18](Cl)(Cl)Cl>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH:18]=[N:17][CH:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1

Participants

4

Reactant 3

HCID 6212ChloroformHCID 7965CyclohexylamineHCID 312444-Methoxybenzaldehyde

Product 1

HCID 10775151123334-93-0

Procedure

A solution of anisaldehyde (21 g) and cyclohexylamine (15 g) in chloroform. (100 ml) was stirred at room temperature for 2 hours and evaporated to afford brown syrup (35 g, quantitative).

Workup

  1. customevaporated
  2. customto afford brown syrup (35 g, quantitative)

Sources & evidence

ORD record
ord-191aa5cf7f2d4e16a2468e329888bf66
Source dataset
uspto-grants-2002_03
Patent number
US06355808B2

Reaction notes

Loading…