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HRID27764

反应详情

EQUATION

反应方程式

HRID 27764 的结构方程式

REACTANTS

反应物

2
结构：NN.O
HCID24654

Hydrazine hydrate (1:1)

H6N2O

结构：CCOC(=O)c1cc(C#N)c(C=O)nc1NC(C)CC
HCID86737220

未命名化合物

PRODUCTS

生成物

1
结构：C=C1NC(NC(C)CC)=C(C(=O)OCC)C(NN)=C1C#N
HCID86737221

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

2.8 g of 5-cyano-6-formyl-2-[(1-methylpropyl)amino]-3-pyridine-carboxylic acid, ethyl ester (0.01 mol) are dissolved in 10 ml of methanol and 1 g of hydrazine hydrate is added with stirring. After standing over night the title compound precipitates. Yield 2.1 g (73%); m.p. 120°-121° C. (methanol).

WORKUP

后处理

  1. waitAfter standing over night
  2. customthe title compound precipitates