1-(2-Methoxyphenyl)piperazine → HCID 22625352, compound

Participants

Reaction Steps

Using 3.88 g of 1-(4-acetoxy-2,3,5-trimethylphenoxy)-2,3-epoxypropane, 3.58 g of 1-(2-methoxyphenyl)piperazine and 100 ml of dioxane, reaction and workup were carried out as in Examples 1-A and 4. After hydrolysis and workup, the residue obtained was recrystallized from benzene-hexane to give 2.06 g of white crystals, m.p. 163-165° C.

Provenance & Evidence