HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 22626826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 22626827 | HCID 22626827 | — |
| Reactant | HCID 22626852 | HCID 22626852 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22626826 | HCID 22626826 | 84.6% |
Reaction Steps
By working in a way similar to that described in example 4 but using (3,5-dichloro-pyridin-4-yl)-acetic acid (1.65 g, 8.026 mmoles), carbonyldiimidazole (1.43 g, 8.829 mmoles), THF (25 ml) and 2-(3-methoxy-phenyl)-8-phenyl-octylamine (2.5 g, 8.026 mmoles), obtained as described in example 13, 3.39 g of the title compound were obtained (yield: 84.6%), m.p.: 97-98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358973B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-d23245bb462343c4bc1ed561d00ed4a4 |
| Source note | uspto-grants-2002_03 |