HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 22626824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22626828 | HCID 22626828 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22626824 | HCID 22626824 | 85.8% |
Reaction Steps
By working in a way similar to that described in example 29 but using LiAlH4 (1.01 g, 26.57 mmoles) in anhydrous ethyl ether (20 ml) and cyclopentyl-(3-methoxy-phenyl)-acetonitrile (5.72 g, 26.57 mmoles), obtained as described in example 32, 5 g of the title compound were obtained (yield: 85.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358973B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-bb4b8b2e402a477eace9d7262a732068 |
| Source note | uspto-grants-2002_03 |