HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 22626839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 22626824 | HCID 22626824 | — |
| Reactant | HCID 22626827 | HCID 22626827 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22626839 | HCID 22626839 | 98.2% |
Reaction Steps
By working in a way similar to that described in example 30 but using (3,5-dichloro-pyridin-4-yl)-acetic acid (2.06 g, 10 mmoles), carbonyldiimidazole (1.78 g, 11 mmoles), THF (30 ml) and 2-cyclopentyl-2-(3-methoxy-phenyl)-ethylamine (2.19 g, 10 mmoles), obtained as described in example 33, 3.8 g of the title compound were obtained (yield: 98.2%), m.p.: 105-106° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358973B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-403b6db1d788429198efa20948520b3a |
| Source note | uspto-grants-2002_03 |