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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 277913Generated: October 29, 2026

1,1'-Carbonyldiimidazole → HCID 22626839, compound

https://huagongshe.com/reaction/277913

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1'-CarbonyldiimidazoleHCID 68263—
ReactantHCID 22626824HCID 22626824—
ReactantHCID 22626827HCID 22626827—
SolventTetrahydrofuranHCID 8028—
ProductHCID 22626839HCID 2262683998.2%

Reaction Steps

By working in a way similar to that described in example 30 but using (3,5-dichloro-pyridin-4-yl)-acetic acid (2.06 g, 10 mmoles), carbonyldiimidazole (1.78 g, 11 mmoles), THF (30 ml) and 2-cyclopentyl-2-(3-methoxy-phenyl)-ethylamine (2.19 g, 10 mmoles), obtained as described in example 33, 3.8 g of the title compound were obtained (yield: 98.2%), m.p.: 105-106° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06358973B1
Source datasetuspto-grants-2002_03
ORD IDord-403b6db1d788429198efa20948520b3a
Source noteuspto-grants-2002_03