HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopropane → HCID 13826357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopropane | HCID 6358 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | (3-Methoxyphenyl)acetonitrile | HCID 88310 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13826357 | HCID 13826357 | 79.9% |
Reaction Steps
By working in a way similar to that described in example 16 but using 3-methoxy-phenyl-acetonitrile (4.4 g, 30 mmoles), anhydrous DMF (40 ml), NaH (55-65%, 1.44 g, 36.3 mmoles) and 2-bromo-propane (4.46 g, 36.3 mmoles), 4.53 g of the title compound were obtained (yield: 79.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358973B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-652326dd20424f0c89c4746a3d50d6b9 |
| Source note | uspto-grants-2002_03 |