1,1'-Carbonyldiimidazole → HCID 22626830, compound

Participants

Reaction Steps

By working in a way similar to that described in example 4 but using (3.5-dichloro-pyridin-4-yl)-acetic acid (5.15 g, 25 mmoles), carbonyldiimidazole (4.24 g, 26.14 mmoles), THF (75 ml) and 2-(3-methoxy-phenyl)-2-phenyl-ethylamine (5.4 g, 23.76 mmoles), obtained as described in example 42, 8.9 g of the title compound were obtained (yield: 85.7%), m.p.: 142-143° C.

Provenance & Evidence