HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 11316133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 22626827 | HCID 22626827 | — |
| Reactant | HCID 22626829 | HCID 22626829 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11316133 | HCID 11316133 | 86% |
Reaction Steps
By working in a way similar to that described in example 4 but using (3,5-dichloro-pyridin-4-yl)-acetic acid (356 mg, 1.73 mmoles), carbonyldiimidazole (308 mg, 1.9 mmoles), THF (15 ml), 2-(2-cyclopentylmethyl-3-methoxy-phenyl)-ethylamine (390 mg, 1.44 mmoles), obtained as described in example 49, and triethylamine (0.24 ml, 1.73 mmoles), 520 mg of the title compound were obtained (yield: 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358973B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-aaf2ee7811ad4f84ae6d102533b0923e |
| Source note | uspto-grants-2002_03 |