HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → Hydroxy[2-(trifluoromethyl)phenyl]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | o-(Trifluoromethyl)benzaldehyde | HCID 123067 | — |
| Product | Hydroxy[2-(trifluoromethyl)phenyl]acetic acid | HCID 101657 | — |
Reaction Steps
The 2-trifluoromethylbenzaldehyde (43.9 g, 252 mmol) was converted to product in a manner substantially analogous to Preparation 59 to yield 39.1 g. (70.5%). EA, MS(FD).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358971B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-65cf0ad731c3423dbd4e46de09a5ec40 |
| Source note | uspto-grants-2002_03 |