HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → Ammonium 3-nitrophthalamidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 3-Nitrophthalic anhydride | HCID 21631 | — |
| Product | Ammonium 3-nitrophthalamidate | HCID 70153617 | — |
Reaction Steps
100 g (518 mmol) of 3-nitrophthalic anhydride were introduced at RT and treated rapidly with 170 ml of concentrated ammonium hydroxide solution with stirring. The mixture was stirred at RT for 1 h. The precipitate was filtered off and dried in a desiccator. Yield: 95.6 g (88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358978B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-653eec6fc0354b73b7a2603e545106bb |
| Source note | uspto-grants-2002_03 |