HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannane, tributyl-1-butynyl- → Methyl 3-benzyloxycarbonylamino-4-(1-butynyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannane, tributyl-1-butynyl- | HCID 11416606 | — |
| Reactant | 2-Benzyloxycarbonylamino-4-methoxycarbonylphenyl trifluoromethanesulfonate | HCID 22627443 | — |
| Product | Methyl 3-benzyloxycarbonylamino-4-(1-butynyl)benzoate | HCID 22627473 | 45.6% |
Reaction Steps
Methyl 3-benzyloxycarbonylamino-4-(1-butynyl)benzoate (646 mg) was prepared from 2-benzyloxycarbonylamino-4-methoxycarbonylphenyl trifluoromethanesulfonate (1.82 g) and 1-butynyl(tributyl)stannane (1.51 g) in a similar manner to that of Preparation 1 (2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358992B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-46410975cdd24aa1b50a5d4b9966df59 |
| Source note | uspto-grants-2002_03 |