4-Methoxybenzaldehyde → HCID 9818097, compound

HRID 278144Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([CH2:11][C:12](O)=O)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH3:15][O:16][C:17]1[CH:24]=[CH:23][C:20](C=O)=[CH:19][CH:18]=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([S:8](/[CH:11]=[CH:12]/[C:20]2[CH:23]=[CH:24][C:17]([O:16][CH3:15])=[CH:18][CH:19]=2)(=[O:9])=[O:10])=[CH:6][CH:7]=1

Participants

Reactant 2

HCID 312444-Methoxybenzaldehyde

HCID 55680(4-Chlorobenzene-1-sulfonyl)acetic acid

Product 1

HCID 9818097HCID 9818097, compoundYield 68%

Procedure

A solution of 4-chlorophenyl sulfonylacetic acid (0.01 mol) and 4-methoxybenzaldehyde (0.01 mol) was subjected to Procedure 1. The title compound was obtained in 68-70% yield.

Sources & evidence

ORD record: ord-81629653c8d44e7a8eeef50f5fa01699
Source dataset: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06359013B1

Reaction notes

Loading…