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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 278265Generated: October 31, 2026

Hydrochloric Acid → HCID 131723149, compound

https://huagongshe.com/reaction/278265

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 21912727HCID 21912727—
SolventMethanolHCID 887—
ProductHCID 131723149HCID 13172314992%

Reaction Steps

A solution of 1-(t-butoxycarbonyl)-4-(1,3-diethyl-4-methyl-(1H)-pyrazol-5-yl)piperidine (348 mg) (from Step E) in 2.5 N HCl in methanol was stirred at rt for 16 h. The solution was concentrated and the resulting solid was suspended in ethyl acetate, filtered and dried to afford 293 mg (92%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06358979B1
Source datasetuspto-grants-2002_03
ORD IDord-1398036eb6344e37bc434aa85c432c23
Source noteuspto-grants-2002_03