HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → n-Neopentanoyl-2-octyldodecylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | 2-n-Octyl-1-dodecylamine | HCID 18761999 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | n-Neopentanoyl-2-octyldodecylamine | HCID 18673285 | — |
Reaction Steps
62 ml of pivaloyl chloride were dissolved in 180 ml of heptane and then added to 150 g of 2-octyldodecylamine at a temperature of 60° C. After addition of 70 ml of triethylamine, the reaction medium was stirred for 2 hours and then purified on silica. 118 g of the desired amide were thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06359175B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-1ca69a6d98714be3b987c3f804e061c4 |
| Source note | uspto-grants-2002_03 |