HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178453612, compound → HCID 178479225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178453612 | HCID 178453612 | — |
| Solvent | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | HCID 178479225 | HCID 178479225 | — |
Reaction Steps
A mixture of 1-(trans-4-tert-butoxycarbonylaminomethylcyclohexane-1-carbonyl)-4-(6-chloronaphthalene-2-sulfonyl)piperazine (0. 7g) and 4 N HCl-ethyl acetate (10 ml) was stirred at room temperature for 1 hour, and the precipitated crystals of the title compound (0.48g) were filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06359134B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-1e1ac8fa1b824492869492b6c0ee0582 |
| Source note | uspto-grants-2002_03 |