HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → 4-[6-(3,5-dimethyl-1H-pyrazol-1-yl)pyridazin-3-yl]morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | HCID 12603548 | HCID 12603548 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-[6-(3,5-dimethyl-1H-pyrazol-1-yl)pyridazin-3-yl]morpholine | HCID 3099054 | — |
Reaction Steps
A mixture of 1.95 g (0.01 moles) of 3-morpholino-6-pyridazinylhydrazine, 1.0 g (0.01 moles) of acetylacetone and 20 ml of ethanol is heated to reflux for 3 hours. After cooling the separated crystals are filtered, washed with ethanol and dried. Yield: 1.65 g (64.5%); m.p. 119°-121° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04224325 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-510458d0ff42413090bb5cb719ecbed0 |
| Source note | uspto-grants-1980_09 |