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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 279154Generated: October 30, 2026

Benzyl Chloride → HCID 22624572, compound

https://huagongshe.com/reaction/279154

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl ChlorideHCID 7503—
ReactantPotassium CarbonateHCID 11430—
Reactant2-Acetyl-1,2,3,4-tetrahydronaphthalen-1-oneHCID 86527—
SolventAcetonitrileHCID 6342—
ProductHCID 22624572HCID 22624572—

Reaction Conditions

Temperature60 °C

Reaction Steps

2-Acetyl-1-tetralone (5.0 g) was added into a mixture of potassium carbonate (3.8 g) and acetonitrile (60 ml). The mixture was stirred at 60° C. for 30 minutes and benzyl chloride was added and the stirring was continued at 60° C. for 5 hours. The mixture was filtered and evaporated. The yield was 7.2 g and was used for further reactions without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06362211B1
Source datasetuspto-grants-2002_03
ORD IDord-f5750697163747a6a3582cd8357d6ae5
Source noteuspto-grants-2002_03