huagongshe.com
HRID279770

反应详情

EQUATION

反应方程式

HRID 279770 的结构方程式

REACTANTS

反应物

2
结构：CCCC[N+](CCCC)(CCCC)CCCC.O=C(N[C@H]1CN(S(=O)(=O)[O-])C1=O)OCc1ccccc1
HCID13575530

未命名化合物

结构：Cc1ccc(S(=O)(=O)[O-])cc1.Oc1cccc2ccc[nH+]c12
HCID23322552

未命名化合物

PRODUCTS

生成物

1
结构：O=C(N[C@H]1CNC1=O)OCc1ccccc1
HCID12834624

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

To a solution of (3S)-2-oxo-3-[[(phenylmethoxy)carbonyl]amino]-1-azetidinesulfonic acid, tetrabutylammonium salt in acetonitrile was added 8-hydroxyquinolinium p-toluenesulfonate. The mixture was refluxed, yielding the title compound as verified by thin layer chromatography (Merck silica gel 60F, ethyl acetate).

WORKUP

后处理

  1. temperatureThe mixture was refluxed