HuagongsheHuagongshe Chemistry Print Report · For research reference only
tetrabutylammonium (S)-3-(((benzyloxy)carbonyl)amino)-2-oxoazetidine-1-sulfonate → benzyl N-[(3S)-2-oxoazetidin-3-yl]carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tetrabutylammonium (S)-3-(((benzyloxy)carbonyl)amino)-2-oxoazetidine-1-sulfonate | HCID 13575530 | — |
| Reactant | 8-Hydroxyquinolinium p-toluenesulfonate | HCID 23322552 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | benzyl N-[(3S)-2-oxoazetidin-3-yl]carbamate | HCID 12834624 | — |
Reaction Steps
To a solution of (3S)-2-oxo-3-[[(phenylmethoxy)carbonyl]amino]-1-azetidinesulfonic acid, tetrabutylammonium salt in acetonitrile was added 8-hydroxyquinolinium p-toluenesulfonate. The mixture was refluxed, yielding the title compound as verified by thin layer chromatography (Merck silica gel 60F, ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04587051 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-ab3570933fde440d99531e40132d99ab |
| Source note | uspto-grants-1986_05 |