HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13608310, compound → HCID 13608303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13608310 | HCID 13608310 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13608303 | HCID 13608303 | — |
Reaction Steps
Dissolve 9.5 g. 3-azido-1-t-butoxycarbonylmethylperhydroazocin-2-one in 85 ml. ethanol. Hydrogenate at 40 psi hydrogen pressure at room temperature using 1.0 g. 10% palladium on charcoal as catalyst. Filter the reaction and concentrate the filtrate to obtain 3-amino-1-t-butoxycarbonylmethylperhydroazocin-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04587050 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-3086a7e1eba74dda82263bc49fc48e51 |
| Source note | uspto-grants-1986_05 |