HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23322533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 23322546 | HCID 23322546 | — |
| Product | HCID 23322533 | HCID 23322533 | — |
Reaction Steps
Saponify this ester with dilute NaOH, acidify the reaction mixture and extract with methylene chloride. After drying and concentration of the extracts, isolate 3-azido-1-(1-carboxyethyl)-perhydroazocin-2-one. Fractionally crystallize this material from acetonitrile as the dicyclohexylamine salt to obtain the desired diastereomer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04587050 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-7e50e9ed9d114b3f9e49955a8d9a383c |
| Source note | uspto-grants-1986_05 |