N,N-Dimethylethylenediamine → HCID 53997976, compound

HRID 27980Notes

Reaction equation

HRID 27980 reaction equation
[CH3:1]N(CCN)C.CN(C)[CH2:9][CH2:10][NH:11][C:12]([CH:14]([OH:32])[C@H:15]1[O:19][C@@H:18]([N:20]2[C:29]3[N:28]=[CH:27][N:26]=[C:24]([NH2:25])[C:23]=3[N:22]=[CH:21]2)[C@H:17]([OH:30])[C@@H:16]1[OH:31])=[O:13]>>[CH2:10]([NH:11][C:12]([CH:14]([OH:32])[C@H:15]1[O:19][C@@H:18]([N:20]2[C:29]3[N:28]=[CH:27][N:26]=[C:24]([NH2:25])[C:23]=3[N:22]=[CH:21]2)[C@H:17]([OH:30])[C@@H:16]1[OH:31])=[O:13])[CH:9]=[CH2:1]

Participants

3

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 54028967adenosine-5'-carboxylic acid N-(2-dimethylaminoethyl)-amide

Product 1

HCID 53997976HCID 53997976, compoundYield 84%

Procedure

with dimethylaminoethylamine: adenosine-5'-carboxylic acid N-(2-dimethylaminoethyl)-amide; m.p. 136°-138° C.; yield 84% of theory.

Sources & evidence

ORD record
ord-310402dfa2b2420b82f5826c743adfae
Source dataset
uspto-grants-1980_09
Patent number
US04224438

Reaction notes

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