HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15068624, compound → HCID 20252039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15068624 | HCID 15068624 | — |
| Reactant | Acetic Acid Mixture with Hydrobromic Acid | HCID 21893785 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20252039 | HCID 20252039 | — |
Reaction Steps
5.0 g. (0.0165 moles) of N-benzyloxycarbonyl-7-chloro-7-cyano-2-azabicyclo[2.2.2]oct-5-ene are dissolved in a mixture of 30 ml. of glacial acetic acid and 15 ml. of a 4-5N glacial acetic acid/hydrogen bromide mixture. The reaction mixture is allowed to stand at room temperature for 10 minutes, and is then evaporated. The evaporation residue is crystallized from acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04587251 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-e31874ef70ca481ba196f82b5c642d33 |
| Source note | uspto-grants-1986_05 |