HuagongsheHuagongshe Chemistry Print Report · For research reference only
Arabinosehydrazon → 1-deoxy-1-hydrazino-D-arabinitol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Arabinosehydrazon | HCID 86740783 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-deoxy-1-hydrazino-D-arabinitol | HCID 53809740 | — |
Reaction Steps
A 1.5 portion of D-arabinose hydrazone in 40 ml of ethanol and 20 ml of water was reduced with 200 mg of platinum oxide and hydrogen for 4 hours. The mixture was then filtered and the filtrate evaporated to dryness. The residue was dissolved in 40 ml of methanol and then evaporated to dryness, giving 1.24 g of 1-deoxy-1-hydrazino-D-arabinitol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04587331 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-03dad06624e54c06b350ad757114f339 |
| Source note | uspto-grants-1986_05 |