Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 4-Nitro-3-phenyl-L-alanine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | L-Phenylalanine | HCID 6140 | — |
| 용매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | 4-Nitro-3-phenyl-L-alanine | HCID 13706 | 43% |
반응 단계
Using the procedure of Bergel and Stock as set forth in J. Chem. Soc., 2409-2417 (1954) L-phenylalanine (50 g) was treated with a mixture of concentrated sulfuric acid (150 ml), and fuming nitric acid (28 ml) to produce the nitro compound Yield 26.9 g (43%) mp 232°-234° C., [α]D25 =+9.6° (c=1.77, 1N HCl).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04587046 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-bcffd1e26f1f46a8acd5510ab76f2131 |
| 출처 메모 | uspto-grants-1986_05 |