N-Methylhomoveratrylamine → HCID 53842786, compound

HRID 280052Notes

Reaction equation

HRID 280052 reaction equation
Cl[CH2:2][CH2:3][N:4]([CH:16]([CH3:18])[CH3:17])[S:5]([C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[C:10]([Cl:15])[CH:9]=1)(=[O:7])=[O:6].[CH3:19][NH:20][CH2:21][CH2:22][C:23]1[CH:32]=[CH:31][C:28]([O:29][CH3:30])=[C:25]([O:26][CH3:27])[CH:24]=1>C1(C)C(C)=CC=CC=1>[CH3:27][O:26][C:25]1[CH:24]=[C:23]([CH2:22][CH2:21][N:20]([CH3:19])[CH2:2][CH2:3][N:4]([CH:16]([CH3:18])[CH3:17])[S:5]([C:8]2[CH:13]=[CH:12][C:11]([Cl:14])=[C:10]([Cl:15])[CH:9]=2)(=[O:7])=[O:6])[CH:32]=[CH:31][C:28]=1[O:29][CH3:30]

Participants

4

Reactant 2

HCID 77039N-MethylhomoveratrylamineHCID 54213297HCID 54213297, compound

Product 1

HCID 53842786HCID 53842786, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

The title compound was prepared by reaction of N-β-chloroethyl-N-(1-methylethyl)-3,4-dichlorobenzenesulfonamide with N-methylhomoveratrylamine in xylene containing inorganic carbonate acid scavengers by heating for five days.

Workup

  1. temperatureby heating for five days

Sources & evidence

ORD record
ord-48aeeb4c59144015aacd504de5209967
Source dataset
uspto-grants-1986_05
Patent number
US04587360

Reaction notes

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