HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 13344548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 53771984 | HCID 53771984 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13344548 | HCID 13344548 | — |
Reaction Steps
20 g of cyclohexyl 2-chloro-4-isocyanatothiobenzoate in 80 ml of toluene were added dropwise to excess aqueous dimethylamine solution at room temperature. The mixture was kept at room temperature, stirred overnight and then filtered under suction. 16.3 g of N-(3-chloro-4-cyclohexylmercaptocarbonylphenyl)-N',N'-dimethylurea (compound no. 35) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588434 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-0ab456e5b979449c90641974acd8c05b |
| Source note | uspto-grants-1986_05 |