HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 280091Generated: October 30, 2026
Thioglycolic Acid → HCID 23321718, compound
https://huagongshe.com/reaction/280091
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | 6-Chloro-1-hexanol | HCID 74828 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 23321718 | HCID 23321718 | — |
Reaction Steps
4.5 ml (0.04M) of 6-chloro-1-hexanol is added to a solution of 2.8 ml (0.04M) of mercaptoacetic acid in 120 ml of 1N NaOH. The solution is warmed to about 50° C. for 16 hours, then acidified and extracted repeatedly with ethyl acetate. The combined extracts are concentrated to dryness and the residue purified by recrystallization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04588718 |
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| Source dataset | uspto-grants-1986_05 |
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| ORD ID | ord-dbb7efea8cf44cce95e82cf72506bc37 |
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| Source note | uspto-grants-1986_05 |
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