HRID280215

反应详情

EQUATION

反应方程式

HRID 280215 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 5-(p-ethoxycarbonylphenyl)-imidazo[1,5-a]pyridine (1.0 g) in 10 ml of ethanol and 10 ml of 1N sodium hydroxide is refluxed for 3 hours. The ethanol is evaporated. The aqueous phase is washed with ether, adjusted to pH=6 and the solid collected to yield 5-(p-carboxyphenyl)imidazo[1,5-a]pyridine.

WORKUP

后处理

  1. customThe ethanol is evaporated
  2. washThe aqueous phase is washed with ether
  3. customthe solid collected