HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Chlorophenyl)-2-oxoacetaldehyde → N-(3-(4-Methylphenyl)propyl)-2-hydroxy-2-(3-chlorophenyl)ethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Chlorophenyl)-2-oxoacetaldehyde | HCID 12463893 | — |
| Reactant | 3-(4-Methylphenyl)propan-1-amine | HCID 12564270 | — |
| Product | N-(3-(4-Methylphenyl)propyl)-2-hydroxy-2-(3-chlorophenyl)ethanamine | HCID 23322149 | — |
Reaction Steps
The title compound was prepared in the manner described in Example 9 using 3-chlorophenylglyoxal and 3-(4-methylphenyl)propanamine. Recrystallisation of the chromatographed material from ether gave the title compound, mp 115°-117.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588749 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-229e1f0bdef4444c9120f96e66be94cb |
| Source note | uspto-grants-1986_05 |