反应详情

The title compound was prepared in the manner described in Example 3 using 2-hydroxy-2-phenylethanamine and 4-ethylphenyl acetone. Recrystallization of the chromatographed material from hexane gave the title compound m.p. 76-82 as a 19:81 mixture of diastereoisomers (analysed as the hemi-hydrate). τ(CDCl3), 8.9 (3H, d, J=6 Hz), 8.8 (3H, t, J=6 Hz), 7.5 (2H, disappears with D2O), 7.0-7.5 (7H, m), 5.35 (1H, dd), 2.9 (4H, s), 2.7 (5H, s).

1. customThe title compound was prepared in the manner
2. customRecrystallization of the chromatographed material from hexane