HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylethanolamine → HCID 18627859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylethanolamine | HCID 1000 | — |
| Reactant | 4-ETHYLPHENYLACETONE | HCID 7019273 | — |
| Product | HCID 18627859 | HCID 18627859 | — |
Reaction Steps
The title compound was prepared in the manner described in Example 3 using 2-hydroxy-2-phenylethanamine and 4-ethylphenyl acetone. Recrystallization of the chromatographed material from hexane gave the title compound m.p. 76-82 as a 19:81 mixture of diastereoisomers (analysed as the hemi-hydrate). τ(CDCl3), 8.9 (3H, d, J=6 Hz), 8.8 (3H, t, J=6 Hz), 7.5 (2H, disappears with D2O), 7.0-7.5 (7H, m), 5.35 (1H, dd), 2.9 (4H, s), 2.7 (5H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588749 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-5d85d69bf2c142818c2bbec3fc9090f9 |
| Source note | uspto-grants-1986_05 |