HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene → Cyclohexane, [(trichlorosilyl)methyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene | HCID 6325 | — |
| Reactant | 1-Methylcyclohexene | HCID 11574 | — |
| Reactant | Trichlorosilane | HCID 24811 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | Cyclohexane, [(trichlorosilyl)methyl]- | HCID 87618 | — |
Reaction Steps
A mixture of 20 ml trichlorosilane, 25 ml chloroform, 8.1 g 1-methylcyclohexene and 0.055 g (phenazine)PtCl2 (C2H4) was refluxed and stirred under nitrogen for 6 days. Distillation of the reaction mixture afforded 2.2 g of trichlorosilylmethylcyclohexane C6H11CH2SiCl3 which was characterized by its mass and NMR spectra.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588800 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-abc6d32437f54e5ab25df4dc23bd3d26 |
| Source note | uspto-grants-1986_05 |